Peer-Reviewed Journal Details
Mandatory Fields
McGlacken, Gerard P; McSweeney, Christina M; O'Brien, Timothy; Lawrence, Simon E; Elcoate, Curtis J; Reen, Jerry F; O'Gara, Fergal;
2010
Unknown
Tetrahedron Letters
Synthesis of 3-halo-analogues of HHQ, subsequent cross-coupling and first crystal structure of Pseudomonas quinolone signal (PQS).
Published
()
Optional Fields
51
45
5919
5921

2-Aryl- and 2-alkyl-quinolin-4-ones and their N-substituted derivs. have several important biol. functions such as the Pseudomonas quinolone signal (PQS) mol. participation in quorum sensing. Herein, we report the synthesis of its biol. precursor, 2-heptyl-4-hydroxy-quinoline (HHQ) and possible isosteres of PQS; the C-3 Cl, Br and I analogs. N-Methylation of the iodide was also feasible and the usefulness of this compd. showcased in Pd-catalyzed cross-coupling reactions, thus allowing access to a diverse set of biol. important mols. The first crystal structure of PQS is also included.

0040-4039
Grant Details